Question: What do respirable silica particles (frac sand pollution) look like?

warren asked on February 22, 2018 17:53
405 views | 2 answers | #15802


We're trying to compile a lot of information about respirable silica particles ( #silica-monitoring ) -- an air pollutant affecting communities near frac sand mines -- as part of the #basic-microscope project to affordably and easily view them through Do-It-Yourself microscopes.

But what do respirable silica particles actually look like through a microscope? It'll be great to have an example to look at at the upcoming event in Wisconsin:

https://publiclab.org/notes/gretchengehrke/02-20-2018/particle-visualization-event-in-hixton-wi



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TXSharon posted this note about photographs of sand dust from a sandbox:

http://www.texassharon.com/2012/07/31/take-this-nice-fracking-sand-for-your-childrens-sand-boxes/

Crystalline silica up close. 1000 times magnification of sand dust sampled from a bag of common playsand. These particles are small enough to be trapped in lung tissue.

SilicaDust.gif

SilicaDust.gif


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This blog is by someone who works for an energy company, helping to mine frac sand, and publishes a book called "Finding Frac Sand" -- yikes.

The image posted is probably of particles way too big to help us that much, but it's interesting to see the color difference and also the note about how acids will dissolve non-silica particles. Maybe there's a way to use their knowledge against them...

http://www.globalenergylaboratories.com/creepy-clowns-terrify-us-all/

I’m talking about impurities in the sand, like iron oxides, clays, feldspars, and carbonates.

These are particles other than the silica sand grains.

These can be seen under the scope, and they tend to be much darker than the pure silica sand. Some are round, which help the sphericity and roundness test.

Here is a microscopic picture of nice silica sand particles next to some impurities and non-silica particles.

Others are nasty jagged creeps.

An additional way to determine how many of these impurities (“creepy clowns”) exist is to perform an acid solubility test.

It’s a very exacting process, using a tight procedure and nasty acid to dissolve the impurities.

So, we are dissolving some of the “creepy clowns” in acid.

It’s kind of satisfying.

As long as the weight dissolved is less than 2% or 3% of the total sample weight (depends on the size of the sand being tested), the sand will meet the American Petroleum Institute standards for frac sand.

silica-sand-and-impurities-not-frac-sand.jpg

silica-sand-and-impurities-not-frac-sand.jpg


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Note these prior questions related to this one:

https://publiclab.org/notes/mathew/10-07-2016/sizing-images-at-portland-science-hackday

And this, where he tries to size a known diameter particle: https://publiclab.org/notes/mathew/08-23-2016/calibrating-a-microscope

https://publiclab.org/questions/gretchengehrke/09-21-2017/is-it-possible-to-accurately-size-inhalable-and-respirable-particles-using-a-diy-microscope

https://publiclab.org/questions/gretchengehrke/09-21-2017/is-it-possible-to-discern-jagged-from-rounded-particles-using-a-diy-microscope

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